About an hour east of Pittsburgh, in Indiana, Pa., inside a windowless building set far back from the road, the scientists at Environmental Service Laboratories test all kinds of things for safety and compliance with regulations, from drinking water to toys to hazardous waste.
The machine that analyzes tap water samples for lead uses a process called inductively coupled plasma optical emission spectroscopy, according to Laboratory Director Gabriel Taylor.
To run the test, a lab tech prepares a tray with 60 different 50 milliliter vials. Some contain calibration samples, some contain quality control samples and some contain customer samples. The instrument has a small robot arm with a long metal tube that sucks the water samples out of the vials and up into the body of the machine.
“It has what’s called a spray chamber, it’s changed into an aerosol, which is basically a vapor,” Taylor said. “It goes up into the machine, the vapor is basically excited by a plasma torch.”
The plasma torch creates an electromagnetic field, which excites the atoms in the sample. Each element will give off a different wavelength of light, and the machine analyzes that light to see if there is lead in the sample and how much.
ESL’s Chief Technology Officer, Angela Chapman, said they calibrate the machine using samples with known amounts of lead each morning. With each batch, they also feed it quality control samples to make sure it’s still on target.
“We add the amount of lead to that water, so we know what it is. We add 10 mg/l to the quality control standard, the instrument processes that standard and then we know we should get back out 10 mg/l of lead, because that’s what we put in it,” Chapman said.
She said each result should be correct within 5 percent, as per Environmental Protection Agency Standards. So if a sample has 10 mg/l of lead in it, the result should be between 9.5 and 10.5 mg/l.
Ten milligrams per liter is 10 thousand parts per billion. The EPA action level is 15 parts per billion, but the highest lead level found in Flint, Mich., was 13,000 ppb. Chapman said it’s important to calibrate the machine to identify those very rare but very dangerous levels of lead.
It takes just 90 seconds to analyze each sample, and about an hour-and-a-half for a whole tray. ESL aims to have results to customers within two weeks of receiving the sample.
Taylor said only about 60 percent of the test kits they send out to customers make it back to the lab for analysis.
“If anybody has a kit laying around at their house and they haven’t sent it in, it might be a good time to send that in, as a reminder,” he said.